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ANALYSIS FOR THULIUM (III) CHLORIDE [LIB]
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Formula : TM1,CL3
Solution chemistry: TM1 +3
All distances below are to the element TM [ thulium ]
| PROTEIN: 2MCP IGA FAB (KAPPA) MCPC603/PHOSPHOCHOLINE
|
Bound Ligands : PC PHOSPHOCHOLINE:
Hev Atom conc.: 75% SATURATION
Precip & conc.: 42.000 % AMMONIUM SULPHATE
Buffer & conc.: 0.100 M IMIDAZIOLE
Addict & conc.: 0.000 M
Comments :
Reference : PADLAN et.al. 1973a:1973b:
pH 7.0 Soak time = Hours Reference number = 66.00
Site 1: 35 GLN L NE2 4.38 ( 8.87) . . .
: 35 GLN L NE2 5.33 ( 9.91) . . .
| PROTEIN: 5TNC TROPONIN-C(TURKEY)
|
Bound Ligands : CA CALCIUM ION IN BINDING SITE III:
Hev Atom conc.: 5.000 mM
Precip & conc.: 39.000 % AMMONIUM SULPHATE
Buffer & conc.: 0.100 M SODIUM ACETATE
Addict & conc.:
Comments : PRESOAK 1.0 HR MODIFIED SLN SOLN I.E. WITHOUT PEG2
Reference : HERZBERG et.al. 1987 :1989 :JAMES et.al. 1985a:1985b:1986 :1988 :
pH 5.0 Soak time = 16.00 Hours Reference number = 9.10
Site 1: 13 PHE CE2 5.96 ( 9.76) . . .
: 90 ALA CB 4.14 ( 5.60) . . H
: 72 HOH O 4.98 (-1.00) . . .
: 104 HOH O 3.62 (-1.00) . . .
: 46 MET CE 5.64 ( 8.28) . . H
: 51 GLN OE1 5.67 ( 4.84) . . .
: 52 ASN O 4.75 ( 5.19) . . .
: 53 PRO CD 5.34 ( 4.96) . . .
: 57 GLU OE2 4.58 ( 8.77) . . H
: 81 MET O 5.94 ( 8.27) . . H
: 82 MET O 5.61 ( 6.96) . . H
: 84 ARG O 5.07 ( 6.52) . . H
: 85 GLN OE1 2.93 ( 2.80) . . H
: 86 MET O 5.76 ( 4.79) . . H
: 87 LYS N 5.91 ( 6.85) . . H
: 88 GLU OE1 5.18 ( 5.42) . . H
: 89 ASP OD1 2.69 ( 4.79) . . H
: 15 HOH O 4.68 (-1.00) . . .
: 42 HOH O 5.78 (-1.00) . . .
: 54 HOH O 5.70 (-1.00) . . .
: 55 HOH O 5.31 (-1.00) . . .
Site 2: 102 PHE CE1 4.40 ( 8.37) . . H
: 106 ASP OD1 5.07 ( 7.27) . s . [Het: CACA - CG 3.50]
: 110 ASP OD1 5.36 ( 6.42) . s . [Het: CACA - CG 3.10]
: 111 GLY O 1.01 ( 3.28) . s .
: 112 PHE CE1 4.46 ( 2.37) . s . [Het: CACA - N 4.10]
: 113 ILE CG1 5.93 ( 5.58) . s .
: 148 ARG CB 5.97 ( 6.93) . s . [Het: CACA - C 3.60]
: 149 ILE O 3.36 ( 5.46) . s .
: 150 ASP OD1 5.83 ( 3.23) . s .
: 151 PHE CB 5.78 ( 5.39) . s H
: 85 HOH O 5.64 (-1.00) . . .
: 106 HOH O 5.73 (-1.00) . . .
: 149 HOH O 3.13 (-1.00) . . .
: 34 GLY O 5.42 ( 5.69) . s .
: 36 ASP OD1 3.44 ( 6.19) . s .
: 72 THR OG1 5.27 ( 6.97) . s .
: 84 HOH O 3.86 (-1.00) . . .