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ANALYSIS FOR LEAD (II) CHLORIDE [DPH]
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Formula : PB1,CL2
Solution chemistry: PB1, +2 : PB1,CL1 +1
All distances below are to the element PB [ lead ]
| PROTEIN: 5CPA CARBOXYPEPTIDASE A/WATER (BOVINE)
|
Bound Ligands : ZN ZINC(II) ION:
Hev Atom conc.: 3.000 mM
Precip & conc.:
Buffer & conc.: 0.200 M LITHIUM CHLORIDE/TRIS/SODIUM CITRATE
Addict & conc.:
Comments : CPA PREP :ALPHA CPA XLS DIALYSING ABOVE SOLUTIONS
Reference : HARTSUCK et.al. 1965 :LIPSCOMB et.al. 1966 :1971 :1973 :REES et.al. 1981 :1983 :
pH 7.5 Soak time = 960.00 Hours Reference number = 228.00
Site 1: 69 HIS ND1 5.65 ( 8.42) . . T [Het: ZNZN - CB 3.40]
: 72 GLU OE1 4.20 ( 7.86) . . T [Het: ZNZN - CD 2.60]
: 127 ARG NH2 5.64 (10.02) . . T
: 196 HIS ND1 5.38 ( 5.95) . . E [Het: ZNZN - CB 3.40]
: 197 SER OG 5.90 ( 4.66) . . T [Het: ZNZN - O 4.00]
: 198 TYR CD1 5.54 ( 4.68) . . T
: 199 SER OG 5.35 ( 6.55) . . T
: 270 GLU OE1 3.16 ( 5.95) . . E
: 279 PHE CE1 4.69 ( 8.48) . . T
: 308 ZN ZN 4.17 (-1.00) . . .
: 567A HOH O 1.15 (-1.00) . . .
: 571A HOH O 2.41 (-1.00) . . .
: 587A HOH O 4.36 (-1.00) . . .
Site 2: 198 TYR O 5.35 ( 7.17) . . T
: 199 SER OG 5.06 ( 7.16) . . T
: 201 LEU CD1 4.92 ( 7.99) . . E
: 203 LEU CD2 5.41 ( 9.22) . . E
: 247 ILE CD1 3.26 ( 6.60) . . T
: 270 GLU OE1 3.31 ( 6.64) . . E
: 567A HOH O 4.04 (-1.00) . . .
: 571A HOH O 4.40 (-1.00) . . .