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ANALYSIS FOR SODIUM HEXACHLOROIRIDATE (III) [AJD]
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Formula : NA3,IR1,CL6
Solution chemistry: IR1,CL6 -3
All distances below are to the element HG [ mercury ]
PROTEIN: 2PAD PAPAIN (CYS DERIV OF CYS-25)
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Hev Atom conc.: 5.000 mM
Precip & conc.: METHANOL/WATER
Buffer & conc.: 0.100 M AMINOETHANOL/HCL
Addict & conc.:
Comments :
Reference : DRENTH et.al. 1962 :1967 :1968 :1971 :
pH 9.3 Soak time = 48.00 Hours Reference number = 129.05
Site 1: 156 LYS NZ 5.45 (10.23) . . T
Site 2: 134 LEU O 5.85 ( 8.20) . . T
: 135 GLN CA 5.94 ( 5.94) . . T
: 136 ALA CB 5.98 ( 5.83) . . T
: 137 ALA CB 3.32 ( 4.20) . . H
: 156 LYS O 4.64 ( 6.73) . . T
: 157 VAL O 5.19 ( 6.14) . . T
: 158 ASP OD1 2.46 ( 3.85) . . T
: 159 HIS CB 5.70 ( 5.92) . . T
: 1 CYS I O 4.06 ( 6.46) d . T
PROTEIN: 2SBT SUBTILISIN NOVO
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Bound Ligands : ACN ACETONE MOLECULE:
Hev Atom conc.: 3.000 mM
Precip & conc.: 55.000 % ACETONE
Buffer & conc.: GLYCINE/NAOH
Addict & conc.:
Comments :
Reference : DRENTH et.al. 1972 :
pH 9.1 Soak time = Hours Reference number = 262.01
Site 1: 128 GLY O 3.34 ( 5.63) . . .
: 129 PRO O 4.70 ( 5.25) . . .
: 130 SER O 5.44 ( 5.24) . . .
: 131 GLY N 5.30 ( 6.09) . . .
: 165 VAL O 2.79 ( 4.99) . . .
: 166 GLY O 2.42 ( 3.39) . . .
: 167 TYR OH 4.33 ( 3.17) . . .
: 168 PRO O 5.90 ( 5.71) . . .
: 169 GLY C 4.83 ( 4.50) . . .
: 170 LYS NZ 3.76 ( 4.96) . . .
Site 2: 25 ASN O 4.97 ( 6.91) . . .
: 27 LYS NZ 3.01 ( 6.12) . . E
: 89 ALA CB 5.41 ( 7.08) . . .
: 91 TYR OH 4.18 ( 9.66) . . E
: 118 ASN O 5.97 ( 7.47) . . .
: 120 ASP OD2 5.97 ( 8.96) . . E
: 183 SER OG 5.80 ( 6.65) . . .
: 185 GLN CD 4.18 ( 5.63) . . .
Site 3: 43 LYS NZ 5.57 (11.57) . . . [Het: ACN CM1 - O 3.50]
Site 4: 52 PRO O 4.41 ( 6.35) . . .
: 53 SER OG 5.39 ( 5.94) . . .
: 16 LEU CD1 5.19 ( 5.85) . . .
: 21 TYR CD1 5.89 ( 6.43) . . .
: 230 ALA O 4.90 ( 5.80) . . .
: 233 LEU CD1 4.80 ( 4.57) . . .
: 234 ILE CD1 5.87 ( 3.84) . . .
: 235 LEU N 5.83 ( 7.12) . . .
: 236 SER OG 5.88 ( 5.96) . . .
: 237 LYS N 5.83 ( 6.60) . . .
: 270 VAL CG1 4.20 ( 5.50) . . .
: 271 GLN N 5.29 ( 5.85) . . .
: 274 ALA O 4.60 ( 5.05) . . .
: 275 GLN O 5.46 ( 6.69) . . .
Site 5: 21 TYR CE1 4.60 ( 6.60) . . .
: 24 SER O 5.42 ( 7.21) . . .
: 232 ALA O 5.76 ( 8.14) . . .
: 233 LEU O 4.94 ( 6.26) . . .
: 234 ILE O 4.43 ( 6.32) . . .
: 235 LEU O 3.44 ( 4.76) . . .
: 236 SER OG 3.47 ( 1.52) . . .
: 237 LYS CG 5.02 ( 2.82) . . .
: 238 HIS ND1 5.92 ( 4.66) . . .
: 239 PRO CD 3.83 ( 5.03) . . .