_____________________________________________________________ 
ANALYSIS FOR POTASSIUM HEXACHLOROIRIDATE (III)       [AJA] 
_____________________________________________________________

Formula           : K3,IR1,CL6                                         
Solution chemistry: IR1,CL6 -3                                         
All distances below are to the element IR [ iridium      ]


PROTEIN:  1CYC CYTOCHROME C (BONITO, HEART)                        


Bound Ligands :  HEM PROTOPORPHYRIN IX CONTAINS FE(II):
Hev Atom conc.: 	  19.000 mM  
Precip & conc.: 	  86.000 %	AMMONIUM SULPHATE                                   
Buffer & conc.: 	          	                                                    
Addict & conc.: 	          	ASCORBIC ACID                                       
Comments      : ASCORBIC ACID; PREVENTS XL AUTOXIDATION             
Reference     : ASHIDA et.al. 1971 :1973 :TANAKA et.al. 1975 :                                                                                                          
pH    6.0   Soak time =    120.00 Hours   Reference number = 256.02  
Site 1:  86  LYS A O     5.96 ( 7.06) . . T  
      :  91  ARG A NH1   4.10 (10.23) . . T  
Site 2:  86  LYS   O     5.23 ( 6.44) . . T  
      :  91  ARG   NH1   3.88 ( 9.98) . . H  


PROTEIN:  1HOE  ALPHA-AMYLASE INHIBITOR HOE-467A (STREPTOMYCES TE  


Hev Atom conc.: 	  10.000 mM  
Precip & conc.: 	  20.000 %	FICOLL 400                                          
Buffer & conc.: 	   0.600 M	SODIUM CHLORIDE/HCL                                 
Addict & conc.: 	          	                                                    
Comments      :                                                     
Reference     : PFLUGRATH et.al. 1986 :                                                                                                                                 
pH          Soak time =    240.00 Hours   Reference number = 215.00  
Site 1:  44  LEU   C     5.69 ( 6.14) . . E  
      :  45  CYS   SG    3.05 ( 4.79) d . E  
      :  73  CYS   SG    4.78 ( 6.10) d . E  
      :  19  ARG   NH1   5.32 (11.55) . . E  
      :   1  ASP   O     4.36 ( 6.77) . . .  
      :   2  THR   OG1   5.68 ( 4.82) . . .  
      :   3  THR   N     5.00 ( 6.09) . . .  
      :   4  VAL   CG2   5.62 ( 7.05) . . .  
      : 101  HOH   O     2.06 (-1.00) . . .